OPTICAL RESOLUTION OF RACEMIC CARBOXYLIC-ACIDS BY GAS-CHROMATOGRAPHY

Authors
MATTRAS H GALZIGNA L PREVIERO A
Citation
H. Mattras et al., OPTICAL RESOLUTION OF RACEMIC CARBOXYLIC-ACIDS BY GAS-CHROMATOGRAPHY, Journal of chromatography, 803(1-2), 1998, pp. 307-310
Citations number
11
Categorie Soggetti
Chemistry Analytical","Biochemical Research Methods
Journal title
Journal of chromatography → ACNP
Volume
803
Issue
1-2
Year of publication
1998
Pages
307 - 310
Database
ISI
SICI code
Abstract
The synthesis of racemic acid amides was performed by using zotriazol- 1-yl-oxy-tris(dimethylamino)-phosphonium hexafluorophosphate as a cond ensing reagent, under mild conditions. The obtained enantiomers are ea sily separated by gas chromatography which yields good resolution for the majority of the products. (C) 1998 Elsevier Science B.V.