Dentin, the inner hard tissue of teeth, is a complex hydrated composit
e and forms the substrate for much of restorative dentistry. Current e
fforts to improve restorative and preventive dentistry involve the dev
elopment of effective bonds to this tissue. Modern bonding techniques
involve etching the dentin to remove the mineral portion, leaving a co
llagen network that can be infiltrated with a monomer and polymerized
in place to form a mechanical bond. The objective of this study was to
investigate the nature of the interfacial zone. called the resin-dent
in interdiffusion zone, using scanning electron microscopy For charact
erization and thickness measurements, X-ray tomographic microscopy for
fracture characteristics and atomic force microscopy for the local mo
dulus and hardness variations. (C) 1998 Acta Metallurgica Inc.