X-ray diffraction is used to investigate YBa2Cu3O7-x (YBCO) films on N
dGaO3(110) and a (100) CeO2/(1 (1) over bar 02) Al2O3, heterostructure
. Symmetric, asymmetric, and axial geometries for theta and theta/2 th
eta scans are used to obtain diffraction spectra from different crysta
llographic planes. The orientational and quantitative twinning charact
eristics of the films are determined. While the crystallographic param
eters of these two types of film (the films are c-axis oriented with c
= 11.67 Angstrom) are similar, there are differences in the twin stru
cture. In particular, the features of the NdGaO3 structure lead to the
appearance of an angle differing from 90 degrees (90.20 degrees) betw
een the possible (110) and (110) twin planes in a YBCO film and a diff
erent number of twin components in each system of twins. It is conclud
ed from an analysis of the broadening of reflections, which are sensit
ive to twinning, that there is not twinning in a 60% film of YBCO on A
l2O3 With a CeO2 buffer layer. (C) 1998 American Institute of Physics.