Y. Chen et al., MECHANICALLY ACTIVATED CARBOTHERMIC REDUCTION OF ILMENITE, Metallurgical and materials transactions. A, Physical metallurgy andmaterials science, 28(5), 1997, pp. 1115-1121
A systematic study of the effect of milling conditions on the low-temp
erature carbothermic reduction of the mineral ilmenite has been carrie
d out. It was found that after ball milling of an ilmenite-carbon mixt
ure at room temperature, the ilmenite was reduced to rutile and metall
ic iron during subsequent low-temperature annealing (760 degrees C for
30 minutes). A longer milling time results in a lower reduction tempe
rature and a higher reduction rate. Higher milling intensity also lead
s to a lower reduction temperature. This enhanced reduction reaction i
nduced by ball milling mainly results from the intimate mixing and lar
ge contact area between milled ilmenite and carbon particles.