A NEW APPROACH TO (9Z)-DODEC-9-EN-12-OLIDE (YUZU LACTONE) VIA PHASE-TRANSFER CATALYSIS CYCLIZATION

Authors
RODEFELD L TOCHTERMANN W
Citation
L. Rodefeld et W. Tochtermann, A NEW APPROACH TO (9Z)-DODEC-9-EN-12-OLIDE (YUZU LACTONE) VIA PHASE-TRANSFER CATALYSIS CYCLIZATION, Tetrahedron, 54(22), 1998, pp. 5893-5898
Citations number
16
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
Tetrahedron → ACNP
ISSN journal
00404020
Volume
54
Issue
22
Year of publication
1998
Pages
5893 - 5898
Database
ISI
SICI code
0040-4020(1998)54:22<5893:ANAT((>2.0.ZU;2-O
Abstract
(9Z)-Dodec-9-en-12-olide (1), also known as ''Yuzu lactone'', a volati le ingredient of Yuzu fruit was prepared in a three step synthesis via Z-selective Wittig olefination, a deprotection and activation protoco l and subsequent cyclization by solid-liquid phase transfer catalysis under avoidance of high dilution conditions. (C) 1998 Elsevier Science Ltd. All rights reserved.