We describe measurements of the electrical resistivity of micron-size
crystallites of boron-doped diamond. Electron-beam lithography was emp
loyed for writing sample-specific contacts on small, well-faceted diam
ond crystals grown by chemical-vapor deposition on silicon substrates.
After generating a three-dimensional computer model of the crystallit
e, a finite-element analysis was used to calculate the internal electr
ostatic potential distribution. Multiterminal resistance measurements,
in conjunction with a computed geometrical factor, enabled the absolu
te resistivity to be determined. We find that the resistivities obtain
ed from two different crystallites agree to better than 10%. The resul
ts are compared with transport measurements on a large-area homoepitax
ial diamond film grown simultaneously with the crystallites. This meth
od can be generalized to obtain electrical transport properties of oth
er small, irregularly shaped samples. (C) 1998 American Institute of P
hysics. [S0003-6951(98)02819-8].