A new method for the measurement of tritium in steel is described. The
method is based on the dissolution of steel in sodium persulfate (per
oxodisulfate) solution, distillation of the resulting solution and mea
surement of tritium in the distillate by liquid scintillation counting
. The method is relatively simple and is capable of reliable determina
tion of tritium in plain carbon steel and 2.25 % Cr, 1% Mo steel at le
vels below 0.1 Bq g(-1).