Ks. Patel et al., NOVEL TECHNIQUE FOR MEASURING THROUGH-PLANE MODULUS IN THIN POLYMER-FILMS, IEEE transactions on components, packaging, and manufacturing technology. Part B, Advanced packaging, 21(2), 1998, pp. 199-202
Polymer thin films are widely used as coatings and interlevel dielectr
ics in microelectronic applications. In multilayer structures, stresse
s generated in the films due to interaction with adjacent layers and s
olvent evaporation induced shrinkage, cause the polymer chains to orie
nt in the plane of the film resulting in anisotropic film properties.
Characterization of properties in all directions is essential for accu
rate electrical and mechanical design and modeling. A new technique ha
s been developed to measure, in-situ, the through-plane (z) stress-str
ain behavior of thin polymer films. A parallel plate capacitor device
and an interdigitated electrode structure were used as sensors to dete
ct changes in dielectric constant and thickness of thin polymer films
under compression. Results are reported for 8-14 micrometer thick, Dow
Chemical Cyclotene 3022 benzocyclobutene (BCB) films, The dielectric
constant was found to change linearly with stress. Using this result,
the through-plane stress-strain curve was obtained.