SYNTHESIS OF TRI(M-SULFONATEDPHENYL)PHOSPHINE (TPPTS) - THE IMPORTANCE OF PH IN THE WORK-UP

Authors
HIDA S ROMAN PJ BOWDEN AA ATWOOD JD
Citation
S. Hida et al., SYNTHESIS OF TRI(M-SULFONATEDPHENYL)PHOSPHINE (TPPTS) - THE IMPORTANCE OF PH IN THE WORK-UP, Journal of coordination chemistry, 43(4), 1998, pp. 345-348
Citations number
13
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
Journal of coordination chemistry → ACNP
ISSN journal
00958972
Volume
43
Issue
4
Year of publication
1998
Pages
345 - 348
Database
ISI
SICI code
0095-8972(1998)43:4<345:SOT(-T>2.0.ZU;2-6
Abstract
Controlling the pH during workup allows synthesis of TPPTS, P(m-C6H4SO 3Na)(3), without interference from the oxide. The recrystallized yield is 70% based on P(m-C6H4SO3Na)(3) . 3H(2)O from PPh3.