NTYL-6-O-TERT-BUTYLDIMETHYLSILYL-BETA-CYCLODEXTRIN AS A CHIRAL STATIONARY-PHASE IN CAPILLARY GAS-CHROMATOGRAPHY

Authors
MIRANDA E SANCHEZ F SANZ J JIMENEZ MI MARTINEZCASTRO I
Citation
E. Miranda et al., NTYL-6-O-TERT-BUTYLDIMETHYLSILYL-BETA-CYCLODEXTRIN AS A CHIRAL STATIONARY-PHASE IN CAPILLARY GAS-CHROMATOGRAPHY, HRC. Journal of high resolution chromatography, 21(4), 1998, pp. 225-233
Citations number
19
Categorie Soggetti
Chemistry Analytical
Journal title
HRC. Journal of high resolution chromatography → ACNP
ISSN journal
09356304
Volume
21
Issue
4
Year of publication
1998
Pages
225 - 233
Database
ISI
SICI code
0935-6304(1998)21:4<225:NAACS>2.0.ZU;2-F
Abstract
ntyl-6-O-tert-butyldimethylsilyl-beta-cyclodextrin has been evaluated as an enantioselective stationary phase for capillary gas chromatograp hy, Experimental results show a good enantioselectivity towards compou nds with different functional groups (haloalkanes, alcohols, esters, t erpenoids, amino acid derivatives, and heterocycles). Column stability improves mixing the chiral phase with polysiloxane SE-54 (1:1).