T. Shizawa et G. Mizuno, DEVELOPMENT OF ONLINE AUTOMATIC ANALYZER FOR INTERFACIAL POLYMERIZATION REACTOR IN POLYCARBONATE PLANT, Kagaku kogaku ronbunshu, 23(3), 1997, pp. 348-352
An on-line automatic analyzer system for an interfacial polymerization
polycarbonate polycondensation reactor has been developed. This analy
zer system has two analyzer units, which are respectively set up for t
wo sections in polycarbonate plant, and moreover the analyzer controll
ing system atilizes DCS (Distributed Control System). One analyzer uni
t is applied for checking oligomer in the first polycondensation react
or and the other is applied for measuring the unreacted raw material i
n the second polycondensation reactor. These analyzer units take advan
tage of titrators, and these units include hydrolysis of oligomer, was
hing of the beaker and, electrode sensor, and are operated by fully au
tomatically. Accuracy of the data obtained by the on-line automatic an
alyzers is equivalent to that of the conventional manual operation. Th
e measured data are calculated by DCS to make the analyzer controlling
system manipulate raw material control valves. This system contribute
s to the stability of quality control, operation, labor saving and imp
rovement of safety of the plant.