Preparation of Standard Reference Material 2383 (Baby Food Composite) and use of an interlaboratory comparison exercise for value assignment of its nutrient concentrations
Ke. Sharpless et al., Preparation of Standard Reference Material 2383 (Baby Food Composite) and use of an interlaboratory comparison exercise for value assignment of its nutrient concentrations, J AOAC INT, 82(2), 1999, pp. 276-287
The preparation of the recently released Standard Reference Material (SRM)
2383 Baby Food Composite and the process used for value assignment of nutri
ent concentrations are reported. SRM 2383 can be used as a control material
when assigning values to in-house control materials and when validating an
alytical methods for measuring proximates, vitamins, and minerals in baby f
ood and similar matrixes. The SRM was prepared as a commercial baby food wo
uld be prepared, with the same ingredients. The Certificate of Analysis for
SRM 2383 provides assigned values for concentrations of proximates, vitami
ns, and minerals for which product labeling is required by the Nutrition La
beling and Education Act of 1990. These assigned values were based on measu
rements by the National institute of Standards: and Technology (NIST) and/o
r collaborating laboratories. Assignment of analyte concentrations based so
lely on analyses by collaborating laboratories is described in this paper.
Certified values are provided for retinol, tocopherols, and several caroten
oids including total beta-carotene the certification of and methodology use
d for measurement of these analytes is discussed in a companion paper (this
issue, page 288). Reference values are provided for solids, ash, fat, nitr
ogen, protein, carbohydrate, calories, vitamin B-1, vitamin B-2, vitamin B-
6, niacin, biotin, calcium, phosphorus, magnesium, manganese, iron, zinc, c
opper sodium, potassium, and chloride. Reference values for addi tional car
otenoids are reported in the companion paper (this issue, page 288). Inform
ation values are provided for iodine, selenium, molybdenum, vitamin D, vita
min B-12, folic acid, pantothenic acid, choline, inositol, sugars, total di
etary fiber and 3 classes of fats.