A vacuum impregnation procedure for examining the microstructure of thermal
spray coatings has been evaluated using a low-viscosity fluorescent resin.
The use of confocal laser scanning microscopy for examining the microstruc
ture allows three-dimensional image reconstruction of the sample. Relations
hips between defects (i.e., porosity or micro/macrocracking) and coating pr
operties can be established more accurately with the proposed methodology b
ecause it enables quantitative analysis.