Using pulse field gradient NMR-based diffusion experiments to identify signals of low-molecular-weight impurities

Authors
Kellenbach, E Burgering, M Kaspersen, F
Citation
E. Kellenbach et al., Using pulse field gradient NMR-based diffusion experiments to identify signals of low-molecular-weight impurities, ORG PROC R, 3(2), 1999, pp. 141-144
Citations number
12
Categorie Soggetti
Organic Chemistry/Polymer Science
Journal title
ORGANIC PROCESS RESEARCH & DEVELOPMENT
ISSN journal
10836160 → ACNP
Volume
3
Issue
2
Year of publication
1999
Pages
141 - 144
Database
ISI
SICI code
1083-6160(199903/04)3:2<141:UPFGND>2.0.ZU;2-K
Abstract
Differences in diffusion rate were utilised to identify signals of low-mole cular-weight impurities in NMR spectra of synthetic pentasaccharide samples using NMR pulse field gradients. This method is of general use to discrimi nate between low-molecular-weight impurities and high-molecular-weight comp ounds in mixtures.