FACILE S-MONODEMETHYLATION OF 3,4,5-TRIS(METHYLSULFANYL)-1,2-DITHIOLIUM IODIDE - CRYSTAL AND MOLECULAR-STRUCTURE OF THE OBTAINED 4,5-BIS(METHYLSULFANYL)-1,2-DITHIOLE-3-THIONE

Authors
SINGH JD SINGH HB DAS K SINHA UC
Citation
Jd. Singh et al., FACILE S-MONODEMETHYLATION OF 3,4,5-TRIS(METHYLSULFANYL)-1,2-DITHIOLIUM IODIDE - CRYSTAL AND MOLECULAR-STRUCTURE OF THE OBTAINED 4,5-BIS(METHYLSULFANYL)-1,2-DITHIOLE-3-THIONE, Journal of chemical research. Synopses, (8), 1995, pp. 312-313
Citations number
12
Categorie Soggetti
Chemistry
Journal title
Journal of chemical research. Synopses → ACNP
ISSN journal
03082342
Issue
8
Year of publication
1995
Pages
312 - 313
Database
ISI
SICI code
0308-2342(1995):8<312:FSO3>2.0.ZU;2-V
Abstract
The reaction of 3,4,5-tris(methylsulfanyl)-1,2-dithiolium iodide with NaBH4 gives a mixture of 4,5-bis(methylsulfanyl)-1,2-dithiole-3-thione 3 (major product) and 2a or 2b (minor product); the crystal structure of 3 is described.