J. Baruchel et al., 1ST TOPOGRAPHIC RESULTS AT THE EUROPEAN SYNCHROTRON-RADIATION FACILITY, Physica status solidi. a, Applied research, 141(1), 1994, pp. 59-69
The first topographic observations performed at the ESRF using the whi
te beam of the ID11 Materials Science wiggler beamline, are described.
Several plate-shaped single crystals (Si, Ge, quartz, Ga- YIG, Fe-3%S
i, Al-Pd-Mn quasicrystals, ...), with thicknesses ranging from 0.3 mm
(Ge) to 1.4 mm (Fe-3%Si) and even 1 cm (Si), are investigated in the t
ransmission mode. The heat load associated with the wiggler beam has t
o be reduced. The main features of the topographs are the short exposu
re times (almost-equal-to 5 x 10(-3) to 10(1) s), the high photon ener
gies corresponding to the recorded Bragg spots (up to almost-equal-to
110 keV), and the good spatial resolution obtained even when setting t
he film far (from 17 cm to more than 1 m) from the sample. The contras
t of dislocation images is consistent with the presently accepted theo
retical models.