W. Pichl et al., MICROPLASTIC RELAXATIONS OF SINGLE AND POLYCRYSTALLINE MOLYBDENUM, Physica status solidi. a, Applied research, 167(1), 1998, pp. 43-60
The microplasticity of high-purity molybdenum single crystals and of M
o polycrystals of technical purity has been investigated by relaxation
step tests in uniaxial compression. A new model for the evaluation of
relaxation tests in the microplastic range of b.c.c metals is present
ed which takes into account the decrease of the mobile dislocation den
sity due to exhaustion of non-screw dislocations. The model allows an
independent determination of the activation volume and of the microstr
ucture parameters controlling dislocation exhaustion. The results indi
cate that in the high-purity single crystals the deformation rate is c
ontrolled by interactions of non-screw dislocations with the grown-in
network. In the Folycrystals additional interactions with impurity ato
ms seem to occur. In the single crystals the activity and subsequent e
xhaustion of two different glide systems was observed, followed by a g
radual onset of screw dislocation motion.