A. Qader et al., TRANSVERSE DISPERSION AND MALDISTRIBUTION IN A PULSED PERFORATED-PLATE EXTRACTION COLUMN, Industrial & engineering chemistry research, 37(6), 1998, pp. 2086-2092
Transverse eddy diffusivities of dispersed phase drops in a 0.30-m dia
meter pulsed perforated plate column were determined by two methods in
volving measurement of changes in local holdup over the column half cr
oss sections, one of which was initially drop free and the transfer of
color tracer over the cross sections, in only one of which tracer was
present initially. Both methods indicated a relatively low diffusivit
y of similar to 10(-4) m(2) s(-1) for both emulsion and intermediate r
egions of operation. However, similar tracer measurements of the radia
l diffusivity for the continuous phase indicated virtually complete mi
xing at the inlet stage. It is concluded that the reduced performance
of these columns with increase in diameter in previous reports must ha
ve been due to initial maldistribution at the dispersed phase distribu
tor at low throughputs, and a proposal is made for a more suitable for
m of distributor.