Cr-Al2O3 and Nb-Al2O3 composites containing 50 vol% metal have been fa
bricated by pressureless sintering of compacts of attrition milled pow
der mixtures. Successful fabrication of high-strength and high toughne
ss composites requires fine and homogeneous powders. Strength and frac
ture roughness of the composites increase with increasing milling time
. Short milling times do not lead to the required particle fineness an
d powder homogeneity. For a composite containing 50 vol% Nb, strengths
of up to 690 MPa with corresponding fracture toughness of 6.6 +/- 0.4
MPa m(1/2) and hardness of 11.2 GPa (H-V20) have been obtained, where
as strengths of 592 MPa, fracture roughness of 6.6 +/- 0.3 MPa m(1/2)
and hardness of 9.3 GPa have been obtained for Cr-Al2O3 composites. (C
) 1998 Elsevier Science Limited. All rights reserved.