ALKOXY-DERIVED FERROELECTRIC PZT FILMS - THE EFFECT OF LEAD ACETATE DEHYDRATION TECHNIQUES AND LEAD CONTENT IN THE ELECTROCHEMICALLY PREPARED SOLUTIONS ON THE PROPERTIES OF THE FILMS

Authors
YANOVSKAYA MI OBVINTSEVA IE SOLOVYOVA LI KOVSMAN EP VOROTILOV KA VASILYEV VA
Citation
Mi. Yanovskaya et al., ALKOXY-DERIVED FERROELECTRIC PZT FILMS - THE EFFECT OF LEAD ACETATE DEHYDRATION TECHNIQUES AND LEAD CONTENT IN THE ELECTROCHEMICALLY PREPARED SOLUTIONS ON THE PROPERTIES OF THE FILMS, Integrated ferroelectrics, 19(1-4), 1998, pp. 193-209
Citations number
14
Categorie Soggetti
Physics, Condensed Matter","Engineering, Eletrical & Electronic","Physics, Applied
Journal title
Integrated ferroelectrics → ACNP
ISSN journal
10584587
Volume
19
Issue
1-4
Year of publication
1998
Pages
193 - 209
Database
ISI
SICI code
1058-4587(1998)19:1-4<193:AFPF-T>2.0.ZU;2-3
Abstract
Different ways of dehydration of lead acetate trihydrate for its appli cation in sol-gel techniques are discussed. Reaction of Pb(CH3COO)(2) . 3H(2)O with acetic acid anhydride proved to be the most efficient wa y of its dehydration. Characteristics of the solutions of lead acetate in methoxyethanol dehydrated by different methods are presented. Solu tions for preparation of PZT films are prepared using electrochemical dissolution of titanium and zirconium in methoxyethanol. Physico-chemi cal properties of these solutions alongside with structural and electr ical characteristics of the PZT films obtained from these solutions ar e presented. The effect of lead content in solutions on the properties of the films obtained is discussed.