TOWARDS HIGHER RESOLUTION FOR QUADRUPOLAR NUCLEI IN SOLID-STATE NMR AT VERY HIGH-FIELD

Authors
MASSIOT D MONTOUILLOUT V MAGNENET C BESSADA C COUTURES JP FORSTER H STEUERNAGEL S MUELLER D
Citation
D. Massiot et al., TOWARDS HIGHER RESOLUTION FOR QUADRUPOLAR NUCLEI IN SOLID-STATE NMR AT VERY HIGH-FIELD, COMPTES RENDUS DE L ACADEMIE DES SCIENCES SERIE II FASCICULE C-CHIMIE, 1(3), 1998, pp. 157-162
Citations number
15
Categorie Soggetti
Chemistry
Journal title
COMPTES RENDUS DE L ACADEMIE DES SCIENCES SERIE II FASCICULE C-CHIMIE → ACNP
ISSN journal
13871609
Volume
1
Issue
3
Year of publication
1998
Pages
157 - 162
Database
ISI
SICI code
1387-1609(1998)1:3<157:THRFQN>2.0.ZU;2-X
Abstract
The recent availability of very high field (800 MHz) and very high mag ic angle spinning rates (35.5 kHz) can lead to important improvements in the field of solid state NMR of half integer quadrupolar nuclei sho wing important or severe second-order quadrupolar broadenings (Al-27, Ga-71...). We give experimental examples of these improvements in the case of both crystalline, defect-bearing and amorphous materials. (C) Academie des Sciences/Elsevier, Paris.