O-Acetyl derivatives of (+/-)-2-furylcarbinols were resolved by PLE ca
talyzed hydrolysis to afford optically active 2-furylcarbinols in up t
o 98% e.e. that are valuable chiral building blocks in the synthesis o
f various biologically active compounds. Enantiomeric excess values we
re determined by using H-1-NMR and GC analysis of (S)-O-acetyllactyl e
ster derivatives of 2-furylcarbinols. They were also correlated with t
he Literature values.