Experimental techniques to measure the thermal properties of solids ar
e discussed. Experimental measurements and parameter estimation techni
ques are used to estimate the thermal properties. The importance of ex
perimental design is emphasized, and criteria that give insight to the
parameter estimation process and experiment are cited. A code-to-code
communication technique is presented, which allows standard stand-alo
ne direct solution programs to be linked with parameter estimation cod
es without modification. This method is called reusable interlace tech
nology (RIT). Aspects of this computational technique are discussed. T
he experimental/computational techniques are demonstrated with an expe
riment to estimate the thermal properties of an orthotropic carbon-car
bon composite material. Two-dimensional, transient temperature and hea
t flux data are used to estimate two components of thermal conductivit
y (in the principal directions of the material) and the volumetric hea
t capacity.