H. Bordet et al., ANALYSIS OF THE MECHANICAL RESPONSE OF FILM ON SUBSTRATE SYSTEMS PRESENTING ROUGH INTERFACES, Thin solid films, 315(1-2), 1998, pp. 207-213
The effect of the mechanical polishing of the substrate surface on whi
ch thin films were deposited was investigated by 'in situ' tensile tes
ts. These tests, performed in a Scanning Electron Microscope, showed d
ifferent responses through cracking and debonding behaviour of the fil
ms, which could be related to the roughness of the substrate surfaces
fixed by the granulometry of the polishing paste. The rougher surfaces
produced an activation of film cracking and debonding earlier than th
e smoother ones. We also observed that the crack activation was depend
ent on the direction of the scratches which were produced before the d
eposition on the samples surfaces. Two directions of scratches were in
vestigated, perpendicular and parallel to the sample tensile axis. A s
imple energy balance gave apparent values of the critical cracking ene
rgy of the film/substrate inter-faces. (C) 1998 Elsevier Science S.A.