Co/Cu multilayers have been grown by electrodeposition using a potenti
ostatic technique in a single electrolyte bath based on CoSO4, H3BO3 a
nd CuSO4. X-ray diffraction performed on these multilayers have shown
polycrystalline fee structure of both Co and Cu layers with preferenti
al (111) texture. Nuclear magnetic resonance spectrum has been recorde
d at 4.2 K on [Co(6 nm)/Cu(4 nm)](25) and has shown a resonance line a
t 216 MHz which confirms the fee structure of Co layers. The analysis
of the spectrum showed on one hand that the Co layers are not pure and
contain approximately 1.5% of Cu, but on the other hand, the interfac
es are of good quality. A cross-sectional on transmission electron mic
rograph showed a columnar growth morphology. Resistivity measurements
performed on this sample presented a giant magnetoresistance (GMR) eff
ect of about 4% at room temperature. (C) 1998 Elsevier Science S.A.