ION ETCHING - STATE-OF-THE-ART AND PERSPECTIVES FOR CONTRASTING THE MICROSTRUCTURE OF CERAMIC AND METALLIC MATERIALS - PART I - DEVELOPMENTAND PHYSICS IN ION ETCHING
I. Graf, ION ETCHING - STATE-OF-THE-ART AND PERSPECTIVES FOR CONTRASTING THE MICROSTRUCTURE OF CERAMIC AND METALLIC MATERIALS - PART I - DEVELOPMENTAND PHYSICS IN ION ETCHING, Praktische Metallographie, 35(5), 1998, pp. 235-254
ion etching has proven itself particularly useful as a method of prepa
ration used for the investigation of special materials. By ion bombard
ement, the surfaces of materials can be etched or removed in a charact
eristic way, ion beam etching of specimens in the electron microscopy
is used, in particular where conventional chemical or electrochemical
thinning techniques fail, such as in examination of microstructures in
metallography and ceramography. In these fields however, only relativ
ely few of the methods for ion etching have been standardised. The pur
pose of this series of articles is therefore to demonstrate the possib
iiities, advantages and disadvantages of this type of etching techniqu
e for metallographical preparation. In the series of articles, the pra
ctical use of the different ion etching techniques is described, toget
her with the theory of ion etching and the effect that the various par
ameters have on the sputtering rate. In these parts of the series, gen
eral views of the historical development and theory of ion etching wil
l be presented and the most important parameter, which can be measured
, the sputtering yield will be explained, This is dependent both on th
e properties of the ions (ion mass, ion energy, ion current density an
d angle of ion incidence), as well as on the properties of the materia
l being etched (crystal structure, surface finish, temperature). The v
arious parameters affecting both the ions and the material itself are
briefly explained.