3 NEW WAYS TO SYNTHESIZE 1,3-AZOLE DERIVA TES UNDER MICROWAVE IRRADIATION

Citation
K. Bougrin et al., 3 NEW WAYS TO SYNTHESIZE 1,3-AZOLE DERIVA TES UNDER MICROWAVE IRRADIATION, Tetrahedron, 54(28), 1998, pp. 8055-8064
Citations number
60
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
ISSN journal
00404020
Volume
54
Issue
28
Year of publication
1998
Pages
8055 - 8064
Database
ISI
SICI code
0040-4020(1998)54:28<8055:3NWTS1>2.0.ZU;2-2
Abstract
Three new ways to synthesize 1,3 - azoles derivatives on mineral suppo rts using Ca(OCl)(2)/Al2O3 or MnO2 / SiO2 or by fusion '' in dry media '' are described. The reactions are activated under microwave irradia tion in a monomode Synthewave 402 reactor. The reaction times are cons iderably shortened and the products are obtained in higher yields and better purity, than compared to conventional heating. (C) 1998 Elsevie r Science Ltd. All rights reserved.