Ld. Wang et al., STUDY ON NANOSTRUCTURAL MORPHOLOGY OF SI3N4 TIN MULTILAYER SYNTHESIZED BY ION-BEAM-ASSISTED DEPOSITION/, Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms, 135(1-4), 1998, pp. 397-400
The structure and morphology of Si3N4/TiN multilayer synthesized by io
n beam assisted deposition (IBAD) were studied by X-ray diffraction (X
RD), Auger electron spectrum (AES) and Field-emmision scanning electro
n microscopy (FESEM). It was found that a well-defined multilayer stru
cture was formed. The multilayer was composed of polycrystalline TiN a
nd amorphous Si3N4. The compositions were determined as N:Ti = 1 and N
:Si = 0.9, respectively. Ion beam etching technique was employed to pr
epare special specimen for FESEM morphology observation. Cross-section
al FESEM was also conducted. Results showed that the Si3N4 layers cons
isted of granular particles of about 100 nm in size and the particles
in TiN layers were much smaller. (C) 1998 Elsevier Science B.V.