S. Kubota et al., WORK-HARDENING BEHAVIOR AND EVOLUTION OF DISLOCATION-MICROSTRUCTURES IN HIGH-NITROGEN BEARING AUSTENITIC STEELS, ISIJ international, 38(5), 1998, pp. 474-481
Microstructural evolution during deformation at room temperature has b
een studied by means of transmission electron microscopy to make clear
the reason for high work-hardening in high-nitrogen bearing austeniti
c steels. Tension tests were carried out at room temperature using thr
ee SUS316L type steels bearing 0.02 to 0.56 mass% nitrogen and 18Mn-18
Cr (retaining ring) type steels bearing 0.51 to 0.84 mass%; nitrogen.
It is found that both yield strength and work-hardening increase with
increasing nitrogen concentration. In high-nitrogen bearing steels, pl
anar dislocation-arrays are formed in the beginning of deformation, fr
equently showing multi-dipoles. Then, they overlap to make dislocation
-walls and at the same time such dislocation-arrays or walls are pinne
d each other presumably by operation of Lomer-Cottrell reaction at the
ir intersections. The dislocation-wall is expected to play a role simi
lar to grain boundary for further deformation. Microstructure observed
in a heavily deformed specimen looks like fine octahedral grid-struct
ure. Thus, dislocation density in a plastically deformed specimen beco
mes much higher in high-nitrogen bearing steels than ina low-nitrogen
bearing steel in which dislocation-cell structure is evolved.