W. Reick et al., RECRYSTALLIZATION-TRANSFORMATION COMBINED REACTIONS DURING ANNEALING OF A COLD-ROLLED FERRITIC-AUSTENITIC DUPLEX STAINLESS-STEEL, ISIJ international, 38(6), 1998, pp. 567-571
Solid state reactions taking place during annealing of 20% cold rolled
ferrite-austenite duplex stainless steel (DIN W.-Nr: 1.4462) have bee
n studied by means of several complementary techniques: optical, scann
ing and transmission electron microscopy, X-ray diffraction analysis,
microhardness and ultramicrohardness measurements and magnetic phase d
etection (ferritoscope). It has been found that after cold rolling aus
tenite exhibited more strain hardening and a higher driving force for
recrystallization than ferrite. Extensive recovery took place in ferri
te during annealing, while the deformation substructure of austenite r
emained nearly unrecovered until beginning of recrystallization. The r
ecrystallization kinetics in ferrite was faster than in austenite. Rec
rystallization in austenite occurred in a more discontinuous manner th
an in ferrite. The eutectoid transformation of ferrite to sigma phase
plus austenite slowed down recrystallization kinetics of both ferrite
and austenite phases. A scheme is presented for sigma phase formation
during recrystallization annealing.