R. Chaim et M. Hefetz, FABRICATION OF DENSE NANOCRYSTALLINE ZRO2-3 WT. PERCENT Y2O3 BY HOT-ISOSTATIC PRESSING, Journal of materials research, 13(7), 1998, pp. 1875-1880
Amorphous to nanocrystalline ZrO2-3 wt. % Y2O3 powders were formed by
chemical precipitation from mixed nitrate salt solutions. The powders
were cold pressed and presintered in air for 2 to 6 h within the tempe
rature range of 1100 degrees C and 1300 degrees C. Hot isostatic press
ing was performed for 2 to 3 h within the temperature range of 1150 de
grees C to 1350 degrees C in argon pressure of 150 MPa. Fully dense pe
llets with grain size of 22 nm to 45 nm were formed by application of
low presintering temperatures.