N. Hayashi et al., FABRICATION OF LARGE SINGLE-DOMAIN SM123 SUPERCONDUCTORS BY OCMG METHOD, Materials science & engineering. B, Solid-state materials for advanced technology, 53(1-2), 1998, pp. 104-108
Melt processing of Sm-Ba-Cu-O bulk superconductors was studied to find
the optimum conditions for fabricating a large single-domain supercon
ductor. First, the holding time at the maximum temperature for the par
tial melting is important for the fabrication of a uniform bulk, espec
ially for a large diameter. When the holding time at the maximum tempe
rature during partial melting was not enough, two separated regions we
re observed, which can be diminished by sufficient holding time. Next
we studied the optimum conditions for grain growth, varying the temper
ature gradient and cooling rate. The processing condition with which w
e have succeeded in growing a single-domain SmBa2Cu3Oy (Sm123 hereafte
r) with dimensions of 35 phi x 15 mm(2) is a temperature gradient of 7
.5 degrees C cm(-1) with a slow cooling rate of 0.33 degrees C h(-1).
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