In this paper a process for the microfabrication of ultrathin (5 nm) f
ree-standing Pt foils is described. A Pt foil is deposited by means of
laser ablation on a Si3N4 membrane covered with a gold layer. This as
sembly is supported by a silicon frame. By electron-beam patterning, i
on milling and plasma etching, the Si3N4 and the gold are removed loca
lly in 1 and 2 mu m-sized square windows. The microstructure of the re
sulting free-standing foils, as studied with HRTEM, is polycrystalline
with crystal sizes ranging from 3 to 15 nm. The foil thickness of 5 n
m is confirmed by electron energy-loss spectroscopy. An application of
such foils lies in the construction of a monochromatic high-brightnes
s electron source, which is based on the ballistic transmission of ele
ctrons through ultrathin foils, using the work function of the foil as
an energy filter. (C) 1998 Elsevier Science B.V. All nights reserved.