Kp. Mingard et al., DIRECT MEASUREMENT OF SPRAYFORM TEMPERATURES AND THE EFFECT OF LIQUIDFRACTION ON MICROSTRUCTURE, Acta materialia, 46(10), 1998, pp. 3511-3521
Citations number
26
Categorie Soggetti
Material Science","Metallurgy & Metallurigical Engineering
Surface temperatures and the corresponding liquid fractions in a spray
deposited commercial 2000 series Al alloy have been measured accurate
ly by plunging thermocouples into sprayforms during growth. Two colour
pyrometry was shown to be reasonably accurate for measuring surface t
emperature but only under constant, or preferably zero, overspray dens
ity. Yield, porosity and grain size have been shown to be strong funct
ions of the top surface temperature and liquid fraction in the sprayfo
rm during spray deposition, over a wide range of liquid fraction. The
final grain size cannot be predicted from the liquid fraction using co
nventional coarsening theories, because they do not take into account
variations in nucleation density and are not applicable at low liquid
fractions. Rapid variation of liquid fraction with top surface tempera
ture during spray deposition implies that to maintain optimum conditio
ns requires control of the temperature to within at least +/- 2 degree
s C. (C) 1998 Acta Metallurgica Inc.