Jh. Gong et Zd. Guan, STRENGTH CRACK-SIZE RELATIONSHIP FOR KNOOP-INDENTED BENDING SPECIMENSAND ITS APPLICATION TO SILICON-NITRIDE CERAMICS/, Journal of the European Ceramic Society, 18(7), 1998, pp. 891-899
With a detailed theoretical analysis, a linear relationship is predict
ed to exist between the fracture strength, sigma(f), and the inverse s
quare roof of flaw depth, (1/a)(1/2), of Knoop-indented bending specim
ens. The effects of residual stresses can be described with a strength
revisionary term of the fitted sigma(f)similar to(1/a)(1/2) equation,
while the fracture toughness can be determined directly from the slop
e term. These predictions are then verified by a variety of tests empl
oyed with a pressureless sintered silicon nitride. Variations of the r
esidual stresses in Knoop-indented specimens with annealing temperatur
e are also explored. It is shown that annealing may not be an effectiv
e method for eliminating the residual stresses in Knoop-indented bendi
ng specimens. (C) 1998 Elsevier Science Limited. All rights reserved.