S. Pant et al., SYNTHESES OF 1,5-BENZOTHIAZEPINES - PART 20 - SYNTHESES OF NOPHENYL)-4-(4-METHOXYPHENYL)-1,5-BENZOTHIAZEPINES, Molecules, 3(6), 1998, pp. 159-163
nophenyl)-4-(4-methoxyphenyl)-1,5-benzothiazepines (5a-e) have been sy
nthesized by reacting 5-substituted-2-aminobenzene-thiols (1a-e) with
4-N-dimethylaminobenzal-4-methoxy acetophenone (2) in dry ethanol satu
rated with hydrogen chloride gas. The products were tested for purity
by tie and characterized by elemental analysis for carbon, hydrogen an
d nitrogen and IR, H-1 NMR and mass spectral studies.