Jh. Bulloch et D. Crowe, EMBRITTLEMENT OBSERVED IN CR-MO TURBINE BOLTS AFTER SERVICE, Theoretical and applied fracture mechanics, 29(1), 1998, pp. 59-66
The present paper describes a study aimed at investigating the extent
of service related embrittlement suffered by a series of Cr-Mo steel t
urbine bolts after over 200,000 h at 450 degrees C. A small section of
material was removed from a noncritical location of all the 51 bolts.
From this section, the chemical composition, average hardness and ave
rage prior austenite grain size were measured. The toughness of the bo
lts was measured by Charpy impact testing and/or Auger electron spectr
oscopy. From the various parameters investigated, it was established t
hat grain size and phosphorus level were the only factors which consis
tently identified whether a bolt was embrittled or non-embrittled. Ind
eed it was established that bolt embrittlement could be predicted usin
g the simple product of microstructure grain size d (mu m's) and bulk
phosphorus content. Finally, it was observed that bolt embrittlement c
ould be predicted using the simple product of microstructure grain siz
e and bulk phosphorus level and that such a trend indicated the import
ance of grain boundary area available for service induced phosphorus s
egregation. (C) 1998 Elsevier Science Ltd. All rights reserved.