My. Huh et al., EFFECT OF LUBRICATION ON THE EVOLUTION OF MICROSTRUCTURE AND TEXTURE DURING ROLLING AND RECRYSTALLIZATION OF COPPER, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 247(1-2), 1998, pp. 152-164
Two polycrystalline copper specimens were deformed by cold rolling wit
h and without lubrication so as to achieve different deformed microstr
uctures. The effect of the different rolling procedures on the evoluti
on of microstructure and texture during rolling and recrystallization
was studied by microstructural observations and X-ray texture analysis
. In addition, local orientations in the as-deformed state were determ
ined by selected area diffraction (SAD) in a transmission electron mic
roscope (TEM) and, after recrystallization, by electron backscattering
diffraction (EBSD) in a Scanning electron microscope (SEM). Whereas t
he rolling textures of the two differently rolled sheets were surprisi
ngly similar, the microstructures strongly differed in so far as the s
ample rolled without lubrication contained a much larger amount of she
ar bands. The present results suggest that the shear component epsilon
(13) caused by friction during dry rolling can effectively be dissipat
ed by shear band formation, resulting in a rather homogeneous overall
rolling texture. With regard to nucleation of recrystallization, shear
bands are known to cut the typical nucleation sites of the cube-orien
tation, the main recrystallization texture component of rolled copper,
but they are also able to act as new nucleation sites. Furthermore, g
rowth of the new recrystallized grains is hindered by the shear bands
because of microstructural and orientation discontinuities at the matr
ix-shear band interfaces. This led to a strong retardation of the recr
ystallization process and gave rise to a very fine grained microstruct
ure and a weak recrystallization texture in the specimen cold rolled w
ithout lubrication. (C) 1998 Elsevier Science S.A. All rights reserved
.