Ag. Drozdetskii et al., PARAMETERS OF SYNTHESIS OF HYDRAZIDES AND 1,2-DIACYLHYDRAZINES BY THERMAL-DECOMPOSITION OF HYDRAZINE SALTS OF ALIPHATIC CARBOXYLIC-ACIDS, Russian journal of applied chemistry, 71(2), 1998, pp. 302-306
zThe reaction parameters were refined for synthesis of hydrazides and
1,2-diacylhydrazines by thermal decomposition of salts of aliphatic ca
rboxylic acids of the general formulas RCOOH . N2H4. H2O and 2RCOOH .
N2H4. H2O (R = C2H5-C8H17). Derivatograms for series of compounds were
obtained. The effect of hydrazine hydrate excess, temperature, reacti
on duration, and crystallization conditions on the yield and quality o
f hydrazides of C-7-C-9 carboxylic acids was studied.