S. Mandl et al., CHARACTERIZATION OF DRILLS IMPLANTED WITH NITROGEN PLASMA IMMERSION ION-IMPLANTATION, Surface & coatings technology, 104, 1998, pp. 161-167
Plasma immersion ion implantation (PIII) is a method which retains the
advantages of conventional beam line implantation while circumventing
the limitations like beam-rastering and target handling for large obj
ects with a complex geometry. However, an electric field which is too
high, especially at small tips or sharp edges, induces arcing, which s
ubsequently damage the implanted workpieces. Here we present investiga
tions performed on high-speed steel drills with a diameter of 0.47 mm
and 8 mm, as well as flat samples, implanted with nitrogen-PIII at dif
ferent voltages between 5 and 25 kV at an elevated temperature of 400
degrees C. For the 0.47 mm drills damage from arcing and subsequent de
crease of the tool cutting life is correlated with the implantation vo
ltage. For the 8 mm drills no detrimental effect of arcing was observe
d and a lifetime increase by 100% was found. The mechanism leading to
this increase is the formation of a very hard compound layer of iron n
itrides followed by a diffusion layer of some 25 I-lm as determined on
the flat samples with hardness, GDOS, and XRD measurements. Further a
nnealing of the samples reduced the surface stress while retaining the
high hardness. (C) 1998 Elsevier Science S.A.