CAPILLARY ELECTROCHROMATOGRAPHY IN COLUMNS PACKED BY GRAVITY - PRELIMINARY-STUDY

Authors
REYNOLDS KJ MALONEY TD FERMIER AM COLON LA
Citation
Kj. Reynolds et al., CAPILLARY ELECTROCHROMATOGRAPHY IN COLUMNS PACKED BY GRAVITY - PRELIMINARY-STUDY, Analyst (London. 1877. Print), 123(7), 1998, pp. 1493-1495
Citations number
20
Categorie Soggetti
Chemistry Analytical
Journal title
Analyst (London. 1877. Print) → ACNP
ISSN journal
00032654
Volume
123
Issue
7
Year of publication
1998
Pages
1493 - 1495
Database
ISI
SICI code
0003-2654(1998)123:7<1493:CEICPB>2.0.ZU;2-I
Abstract
Chromatographic material was delivered into fused silica capillary col umns mainly by the use of sedimentation by gravity. After sedimentatio n of the packing material, the columns were pressurized at 8000 psi an d evaluated for capillary electrochromatography (CEC). The capillary c olumns were tested using a commercially available capillary electropho resis unit. Under typical CEC conditions, the capillary columns packed by gravity showed reduced plate heights below 2 with a reproducibilit y of less than 9% RSD.