T. Kingetsu et al., HIGH-TEMPERATURE PHASE AND MORPHOLOGICAL-CHANGES OF CVD-SIC FILMS STUDIED USING IN-SITU X-RAY-DIFFRACTOMETRY, Materials letters, 36(5-6), 1998, pp. 284-289
Phase and morphological changes of polycrystalline, chemical-vapor-dep
osited beta-SiC films on graphite at temperatures up to 2500 degrees C
were investigated by in situ X-ray diffractometry (XRD). It was demon
strated that MID using imaging plate was useful for monitoring the cha
nges: the beta-SIC transformed into alpha-SiC at 2200 degrees C and th
en decomposed and were sublimated to develop protruding dendrite struc
tures of beta-SiC on the surface because of temperature gradient there
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