A ROUND-ROBIN EXPERIMENT OF ELEMENTAL SENSITIVITY FACTORS IN LOW-ENERGY ION-SCATTERING

Citation
Hh. Brongersma et al., A ROUND-ROBIN EXPERIMENT OF ELEMENTAL SENSITIVITY FACTORS IN LOW-ENERGY ION-SCATTERING, Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms, 142(3), 1998, pp. 377-386
Citations number
19
Categorie Soggetti
Instument & Instrumentation","Nuclear Sciences & Tecnology","Physics, Atomic, Molecular & Chemical","Physics, Nuclear
ISSN journal
0168583X
Volume
142
Issue
3
Year of publication
1998
Pages
377 - 386
Database
ISI
SICI code
0168-583X(1998)142:3<377:AREOES>2.0.ZU;2-J
Abstract
In a round robin experiment a set of five polycrystalline, metallic sa mples is studied by low-energy ion scattering (LEIS) in five different laboratories, The energy range is 0.6-3.5 keV and He and Ne ions are used. Even though different experimental setups are used the evaluated elemental sensitivity factors agree within +/-20%. Reproducibility wi thin single laboratories is better than 10%. In an additional study ca rried out in three laboratories the surface composition of an alloy, C u55Pd45, was determined, using in situ calibration standards, These su rface composition measurements agreed within +/-3 at% demonstrating th at quantitative composition determination is possible using this proce dure. (C) 1998 Elsevier Science B.V. All rights reserved.