Rj. Mcdonald et al., RAPID DETAILED CHARACTERIZATION OF CONCRETE SHIELDING BLOCKS UTILIZING INTERNAL NATURAL RADIONUCLIDES FOR CALIBRATION, Journal of radioanalytical and nuclear chemistry, 233(1-2), 1998, pp. 191-194
Following many years of productive research, the 184-inch Cyclotron, t
he SuperHILAC, and the BEVALAC accelerators at the Berkeley Laboratory
were closed, leaving thousands of concrete shielding blocks available
for reuse, recycling, or disposal. The process history of these block
s precludes free release pending radiological characterization. This p
aper describes a procedure whereby a high efficiency shielded germaniu
m spectrometer is used to rapidly characterize natural and man-made ac
tivity within the blocks. The spectrometer is moved up to the block an
d 5 minutes of data are collected at the point on the block that regis
ters highest on a micro-R meter. Sensitivity is better than 1 pCi/g (0
.037 Bq/g) for Co-60 and Eu-152, the prominent man-made activities obs
erved. One-time calibration of the detector system is obtained from a
sample of concrete, drilled with a hammer drill, counted in our low-ba
ckground facility, and compared to crushed rock with known U, Th, and
K activity. A simple relationship exists between the counts/minute obs
erved in a characteristic gamma-ray peak and the activity in the block
.