T. Tamiya et al., IN-SITU OBSERVATIONS OF R-PHASE TRANSFORMATION IN A TI50NI48FE2 ALLOYBY ELECTRON-MICROSCOPY, Materials transactions, JIM, 39(7), 1998, pp. 714-723
The R-phase transformation In a Ti50Ni48Fe2 alloy was studied by in-si
tu electron microscopy with double-tilt cooling stages and an energy-f
ilter, and the controversial Incommensurability in the early stage of
the transformation was examined by using imaging plates, which have hi
gh sensitivity and are easy to access to computer analysis. As a resul
t, the transformation was shown to proceed in the following way. The R
-phase transformation starts at R-s point, where the electrical resist
ance starts to increase, from the B2 parent phase with weak diffuse sc
attering to the commensurate R-phase with a sharp interface. Thus, the
transformation is a first order throughout, and the temperature hyste
resis represents the two-phase region of the B2 parent and Ii-re comme
nsurate R-phase.