Jk. Chen et al., INTERFACIAL STRUCTURE AND GROWTH MECHANISMS OF LATH-SHAPED PRECIPITATES IN NI-45 WT-PERCENT CR, Philosophical magazine. A. Physics of condensed matter. Structure, defects and mechanical properties, 78(2), 1998, pp. 405-422
The interfacial structure of bcc laths precipitated from a nickel-rich
fee matrix were studied using transmission electron microscopy and hi
gh-resolution electron microscopy (HREM). 50 precipitates and more tha
n 200 defects in their vicinity were analysed. HREM images indicate th
e parallel conjugate planes of the Kurdjumov-Sachs orientation relatio
nship are continuous across the broad face of the laths. In agreement
with earlier studies, the (1 (2) over bar 1)(f) habit plane contains s
tructural ledges, irregularly spaced dislocations but no regular array
of misfit dislocations. 87% of dislocations in the habit plane have B
urgers vectors in the conjugate plane. These dislocations are found in
the risers of growth ledges and must climb as the ledges migrate. The
dislocations accommodate misfit in the conjugate planes of the orient
ation relationship while misfit perpendicular to these planes is compe
nsated by elastic strain. Stacking faults found extending into the mat
rix from the precipitate habit plane accommodate elastic strain and ap
pear to aid the formation of growth ledges. On the side facet of the p
recipitate lath, two types of linear defect are found misfit dislocati
ons spaced 12 nm apart with 1/3[1 (1) over bar 1](f) Burgers vectors,
and structural ledges parallel to the misfit dislo$iions spaced 1.5 nm
apart. The misfit dislocations are in a sessile orientation with resp
ect to growth of the side facet.