A. Griffo et al., STATISTICAL-ANALYSIS OF LUBRICANT PARTICLE-SIZE EFFECTS ON FERROUS P M ALLOYS/, International journal of powder metallurgy, 34(5), 1998, pp. 55-65
Ferrous powder metallurgy is among the largest commercial activities i
n P/M and ferrous alloys have been studied widely in terms of alloying
effects and sintering environments. One major processing step that ha
s been ignored in general is the lubricant effect on compaction and af
ter sintering. Several prior studies compared different lubricants, su
ch as zinc stearate and ethylene bisstearamide, but no study has evalu
ated quantitatively the role of lubricant particle size. This study ev
aluated statistically a 3(4) matrix using green and sinter response va
riables to isolate the lubricant particle size effect. The statistical
analysis assures credibility of the reported results. Three ethylene
bisstearamide lubricants, three loading levels, three compact pressure
s, and three ferrous P/M alloys were selected for the basis of the exp
erimental matrix. The study concluded that a statistical difference ex
ists for measured response variables, including dilation, hardness, an
d density. The differences are small, however for most scenarios. The
results indicate that lot-to-lot variations in lubricant particle size
will not effect sintered properties significantly.