This paper discusses the photoluminescence and x-ray microstructural p
roperties of epitaxial layers of solid solutions of InGaAsP isoperiodi
c with InP (100) and GaAs (100) substrates, obtained in the region of
immiscibility and spinodal decay. It shows that there is good agreemen
t of the experimental results with the theoretical model of spinodal d
ecay. The boundaries of the region in which two solid phases of differ
ent composition exist in epitaxial layers of solid solutions of InGaAs
P isoperiodic with the InP and GaAs substrates are determined. A perio
dic nanoheterostructure is obtained in an epitaxial layer of InGaAsP s
olid solutions with a repetition period of 650 +/- 30 Angstrom in two
mutually perpendicular directions. (C) 1998 American Institute of Phys
ics.