P. Revel et al., EXPERIMENTAL SIMULATION OF A MARTENSITIC STAINLESS-STEEL COATING SUBJECTED TO THERMAL FATIGUE, Revue de métallurgie, 95(5), 1998, pp. 679-690
Studies of thermal fatigue damage have been an area of ever-growing in
terest in the industries such as aerospace, nuclear, metallurgy and ot
her industries where metallic structures have been subjected to thermo
mechanical loadings. Thermal fatigue effects will only be evident, if
the thermal cycled structure size is big enough. In this work, we have
studied continuous cast cylinders which are components submitted to t
hermal cycles. The repetition of temperature cycles induces many fract
ures on material surfaces and could induce cylinder failure. In order
to attempt to solve this important technological problem by protecting
the surface, a coating was deposited on the cylinder by a semi-transf
erred plasma are technique; this method provides a coating which is no
t too diluted into the support. In the present work, a martensitic sta
inless steel was deposited on a cylindrical low alloyed steel substrat
e, simulating a true cylinder; the specimen used in this study has dim
ensions of a 1/5 of those of a real cylinder. It was high frequency he
ated with a pancake type inductor and cooled with a compressed air sys
tem on its outer surface and an axial flow cooling water inside; the s
pecimen was rotated at a speed of 1.1 R.P.M. An experimental temperatu
re map was established using two infrared pyrometers for temperature s
urface measurements and Thermocouples for infernal temperature measure
ments; these were inserted into the cylinder. The objective of this tr
idimensional simulation is to obtain the best reproduction of thermal
loading of the casting cylinder, When the thermal stabilized cycle is
reached (after 15 cycles), twenty temperature measurements were carrie
d out in order to construct the experimental thermal map of the stabil
ized cycle, Furthermore, different experimental maps were constructed
from the initial state to the stabilized cycle. The temperature range
was established to correspond to typical industrial values, and moreov
er, the experimental thermal maps will be used to a future numerical s
imulation of the thermomechanical behaviour of the cylinder. The highe
st measured temperature was 500 degrees C close to the inductor; the l
owest temperatures were measured near the axis at 40 degrees C and als
o at the end of a generating line at 180 degrees C. Furthermore, resid
ual stresses and deformations were measured in the coating depth befor
e the thermal fatigue experiment and at different periods of the test.
These measurements were performed using X Ray and neutron diffraction
, before and after thermal fatigue cycles. Experiments performed on cy
lindrical specimens are difficult and expensive; thermal fatigue tests
serve only for the verification of the coating toughness and for the
construction of thermal maps. The study of the microstructural evoluti
on of the coating was conducted with the help of other smaller specime
ns, which were submitted to thermal shocks;some microhardness measurem
ents were carried out to estimate hardness variations of the coating.
These specimens are small coated cylinders; their thermal cycles were
identical with thermal fatigue cycles. Moreover, the temperature evolu
tion of the specimens was adjusted in order to correspond to the therm
al evolution of the thermal fatigue coating cylinder. However, only a
numerical simulation of these thermal shock experiments will allow to
evidence the balance between this simplify test and the thermal fatigu
e test. After 150 fatigue thermal cycles, no cracks were observed on t
he surface of the cylinder. After 100 additional cycles, with a new hi
gher temperature of 700 degrees C, no damage was evident on the surfac
e. Residual stresses decrease quickly with thermal cycles; decreases i
n hardness were also correlated with lower yield points. Several isoth
ermal mechanical tests were performed on the coating material (low cyc
le fatigue and relaxation) and on the support to determine their therm
omechanical behaviour in the temperature range 20-700 degrees C. The p
arameters were identified by means of a systematic numerical procedure
(a computer program of simulation and identification). The microstruc
tural evolution, during mechanical tests, was examined and related to
the evolution of internal variables of the viscoplastic model. It was
found that, at every temperature, the material showed cyclic softening
behaviour. Moreover at 450 degrees C, a high stress level was correla
ted with the evolution of the material microstructure and the increase
of the kinematic variables of the model. The viscoplastic model chose
n in this study permits a good description of, not only the macroscopi
c mechanical results, but also of the microstructural evolutions of th
e material, An anisothermal constitutive model could be introduced int
o a numerical procedure; the latter, with the aid of a finite element
method, should permit the calculation of the thermomechanical effects
of thermal fatigue on structures such as cylinders. It should also per
mit a comparison between the two tests of thermal fatigue and thermal
shocks.