PHTHALONITRILES BY HETERO-DIELS-ALDER REACTIONS OF 4,5-DICYANOPYRIDAZINE WITH ENAMINES - ISOLATION AND CHARACTERIZATION OF UNPRECEDENTED INTERMEDIATES

Citation
R. Nesi et al., PHTHALONITRILES BY HETERO-DIELS-ALDER REACTIONS OF 4,5-DICYANOPYRIDAZINE WITH ENAMINES - ISOLATION AND CHARACTERIZATION OF UNPRECEDENTED INTERMEDIATES, Tetrahedron, 54(36), 1998, pp. 10851-10856
Citations number
12
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
ISSN journal
00404020
Volume
54
Issue
36
Year of publication
1998
Pages
10851 - 10856
Database
ISI
SICI code
0040-4020(1998)54:36<10851:PBHRO4>2.0.ZU;2-A
Abstract
The title conversions were shown to involve as key intermediates new d icyanodiene systems, that can be isolated in high yields under mild co nditions; their structures, inferred from analytical and spectral data , were confirmed by an X-ray study. Some improvements for the syntheti c methodology connected with this finding are discussed. (C) 1998 Else vier Science Ltd. All rights reserved.